<small id="f2xv5"></small>

  •
    • <cite id="f2xv5"></cite>

        



        
  
        
  	
        
    	
        德思特生物專注于中藥（植物藥）物質基礎研究以及天然化合物、中藥化學對照品實物生產供應
        
        
    
        
  
        
  
  
        
	
        
    
    

        天然藥物活性單體及中藥對照品專業生產供應商

        
    
        聯系方式
        028-85003950
        
    
        
   
        
   
   
        
   	  
    
        

        



        
	
        
		
	
        

        




        
	
        
   	  
    


        
        
        
        	
        
        		
                
                
                
                
        
                	
        聯系方式
        
                	
        
                    	
        服務熱線：
        028-8500-3950
        公司傳真：028-85589956
        公司郵箱：sales@tcmlmt.com
        公司網址：m.chuaihan.com
        公司地址：四川省成都市溫江區?？坡肺鞫?28號5棟

                            
        
                
        
                
        	
        
            
        
            
        		
        
                	  
        
                        
        發表文獻展示
        
                        當前位置:首頁關于德思特 > 發表文獻展示 > 
                      
        
                      
        
                   		  
        
                   		  		
        Journal of separation science-03 March 2019 京尼平苷酸 梔子苷
        
                   		  		
        時間：2020-09-03   瀏覽次數：  分享到：
        
                   		  			
        
                   		  		
        
                   		  		
        
                   		  			Ionic liquid vortex-simplified matrix solid-phase dispersion for the simultaneous determination of terpenoids, crocins, quinic acid derivatives and flavonoids in Gardeniae fructus by UHPLC
        
期刊名：Journal of separation science
        
文獻編號：DOI 10.1002/jssc.201801354
        
文獻地址：https://onlinelibrary.wiley.com/doi/abs/10.1002/jssc.201801354
        
發表日期：03 March 2019
        

        
Abstract
        
A novel ionic‐liquid‐based vortex‐simplified matrix solid‐phase dispersion method using 2,6‐dimethyl‐β‐cyclodextrin was established by ultra high performance liquid chromatography coupled with a photodiode array detector. 2,6‐Dimethyl‐β‐cyclodextrin was first used as a promising adsorbent in this proposed method for simultaneous determination of eight compounds in Gardeniae fructus. These compounds are terpenoids (geniposidic acid, genipin‐1‐β‐D‐gentiobioside, geniposide, 8‐o‐acetyl shanzhiside methyl ester), crocins (crocin‐I, crocin‐II), quinic acid derivatives (chlorogenic acid), and flavonoids (isoquercitrin), respectively. Several parameters were investigated in the adsorption and desorption processes to obtain the optimal conditions, including 2,6‐dimethyl‐β‐cyclodextrin as sorbent, 0.5 mL 100 mM 1‐dodecyl‐3‐methylimidazolium hydrogen sulfate as the extraction solvent, 2:1 of sample/sorbent ratio, grinding for 2 min and vortexing for 60 s. The recoveries of the eight compounds ranged from 96.6 to 100% (<3.50%). The limits of detection and quantification were in the range of 0.02–0.30 and 0.06–1.25  μg/mL, respectively. Meanwhile, a good linearity was attained with r values (>0.9997). The established method showed higher extraction efficiency and less reagent consumption than traditional matrix solid phase dispersion and ultrasonic‐assisted extraction. Hence, it could be applied for sample preparation and analysis of natural products.
        

        
Standard substances including geniposidic acid, chlorogenic acid, genipin-1-β-Dgentiobioside, geniposide, 8-o-acetyshanzhiside methyl ester, isoquercitrin, crocin I, and crocin II were purchased from Chengdu Desite Biological Technology Co., Ltd(Chengdu, China).                   		  		
        
                   		  		
                   		  
        
                      	  
                      
        
                
        
                
                
        
                	
        
                        
        熱門新聞
        
                    
        
                    
        
                        					                                                  
        
                            
                            
        
                                
        Afrormosine CAS:550-79-8 中藥對照品標準品
        
                                
        產品編碼：DA0040產品名稱：Afrormosine英文名:AfrormosineCAS登錄...
        
                                查看更多
                            
        
                        
        
                        
          
                                                   
        
                                                                    
        
                    
                    
                
        
                
        	
        
        
        
        
    
        

        










        
	
        
	
        
        
        
        
    
        

        


        
	
        
		
    
        
    
        
		
        
		 
        德思特
        
		 
        
		 	版權所有：成都德思特生物技術有限公司 Copyright © 2016   蜀ICP備16023840號-2
        
公司地址：四川省成都市溫江區海科路西段128號5棟
        
公司電話：028-85003950
        

        
		 
        
		 
        掃一掃關注德思特
           掃碼關注公眾號
         
        
		
        		
	
        	

        
 
     
     
     
     





四虎国产永久免费久久_狠狠躁夜夜躁人人爽天天30人_成人动漫在线免费观看_久久婷婷激情综合色综合俺也去

        <small id="f2xv5"></small>
      2. 

        

        4. <cite id="f2xv5"></cite>